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Heating contines... 9) ... and take another plate after 2 h 30 min, but to mix things up I decide to try a different eluent, Make one with 5 mL DCM and 0.2 mL MeOH. The DCM pulls the Be spot too high, This eluent mixture was more polar than hexane and ethyl acetate one. 10) After 3h TLC shows that much 3,4,5-TMBA remains, so at 3 h 20 min add 30 mL more NM. 11) Made a few more TLC plates and finally after about 7 hours of the reaction running between 50 — 60...