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Une solution CuCl2 (105 g) dans de l'eau (200 ml) est lentement ajouté goute à goute pour garder la mixture en dessous de 80 °С. La réaction est ensuite conservé à 80 °C pour 30 minutes avec l'aide d'un radiateur externe. NaOH (8 liters 25%) en solution aqueuse se rajoute à la réaction chimique et les couches sont séparées.
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