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Smoke or some sort of mist forms on the surface of the reaction mixture after addition of MEA, suck it away. 8) Take TLC after 1 h 45 min and it does seem to show two spots with some sort of product, a tail above the 3,4,5-T MBA, but there is clearly lots of unreacted BA left. Heating contines... 9) ... and take another plate after 2 h 30 min, but to mix things up I decide to try a different eluent, Make one with 5 mL DCM and 0.2 mL MeOH.